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Showing 3 results for Xrd

Nima Nezafati, Morteza Hessari,
Volume 1, Issue 1 (4-2017)
Abstract

The East Chia Sabz site is located at the bank of the Seymareh river in the middle of Zagros Mountain chain. The site is among the few collections of the Acramic Neolithic sites of eighth millenium BCE of Zagros which was archaeologically investigated during the rescue archaeological studies of the Seymareh dam. Numerous bullet-shaped core stones were unearhted during the archaeological excavation of the site, from which some were investigated using XRD analysis. According to the results, most of the lithic artifacts demonstrate a similar mineralogy and it seems that they had been provided from a local source. In this regard, the silisic cobbles of the Amiran Formation that are also available from the river beds could have been a significant source.

Elahe Pourabdollah,
Volume 4, Issue 1 (10-2021)
Abstract

Pigments play a crucial role in identifying the authenticity of historical and cultural artworks and hold a special position in conservation and restoration practices. Among them, recognizing the methods of identifying pigments used in historical manuscripts plays a significant role in determining the identity and authenticity of these artifacts. This study aims to review various methods of identifying pigments employed in historical manuscripts. Investigations in this paper have been conducted using non-destructive analytical techniques such as Scanning Electron
Microscope with Energy Dispersive X-ray Spectroscopy (SEM-EDX), Fourier Transform Infrared Spectroscopy (FTIR), X-ray Fluorescence (XRF), X-ray Diffraction (XRD), Polarized Light Microscopy (PLM), Particle Induced X-ray Emission (PIXE), Atomic Force Microscopy (AFM), micro-Raman spectroscopy, and optical imaging for elemental and compositional identification of pigments. Among these methods, SEM-EDX and point analysis
have been more commonly used in identifying historical pigments. Additionally, the combination of multiple techniques can be a suitable solution for identification purposes, but depending on the purpose of identification and the sensitivity of the artifact, factors such as the feasibility of on-site analysis or transferring artifacts to various laboratory facilities, using non-destructive methods, the possibility of sampling, and the significance and value of the artifact should be considered to adopt the best possible method. If necessary, combining tests and instrumental methods can lead to a more accurate understanding of pigments alongside their chemical composition.

Sana Kazemzad Bagha, Mahdi Razani,
Volume 5, Issue 1 (3-2022)
Abstract

 The following article aims to conserve and restore a part of the rock door and stone tower of the Pasargad World Heritage Site. The rock piece belongs to the right wing of the stone tower and is decorated with six lotus flowers. This object had much damage that caused the preservation and protection of the work to problems such as fracture and lack of integrity. Therefore, the restoration practice started on the stone piece. The best intervention method is selected after the historical, physical, and chemical knowledge of the effect. In this regard, studies have been conducted in the field of knowing and investigating the political history, architecture, nature, and use of the rock tower, and instrumental analyses such as petrography, X-ray diffraction (XRD), X-ray fluorescence (XRF) have been performed to identify the physical and chemical dimension of the object. The results show that the work belonged to the stone tower and was probably built during the reign of Darius. The rock used to build the artefact is dolomitic limestone. Finally, with the help of the mentioned analyses and according to the restoration principles of restoration, practical procedure, and preventive conservation were carried out on the stone piece. Finally, the work was placed inside a frame made of Teflon sheet for display so that the work has both visual integrity and can be reversed for future restorations.


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