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Showing 4 results for Sem-Edx

Arman Razm, Hossein Ahmadi, Abbas Abed Esfahani ,
Volume 1, Issue 2 (10-2017)
Abstract

Many artifacts found in the places where ancient communities lived in Jurjan indicate the antiquity of life in this region. Much evidence of Jurjan's importance in historical periods, including the Achaemenid, Sassanid, and Seleucid periods, can be found in inscriptions from that period. During the Seljuk period, Jurjan was the cradle of science, literature, art, and industry in northern Iran, and was one of the country's important centers for glassmaking, pottery, and metalworking, and the use of glazes on pottery. The use of black patterns and turquoise glazes is abundant in pottery objects excavated in Jurjan. In this study, three samples of pottery with this type of glaze in the Jurjan region were examined in terms of technology, and the manufacturing method and materials used in them were studied. In this regard, the glazes were identified using digital microscopy, polarizing optical microscopy, scanning electron microscopy, and X-ray diffraction analysis. According to microscopic images of the cross-sections of the samples, the glazing method is underglaze and three layers are visible to create the glaze. First, a milky layer called engobe is created on the surface of the pottery, then black patterns are applied on it, and finally a layer of transparent turquoise glaze covers the entire surface.

Masoud Bagherzadeh Kasiri, Sepideh Naghibi,
Volume 2, Issue 1 (6-2019)
Abstract

Studying various aspects of the manuscripts may be important in explaining the actual values of work, and the ways of protecting these values. Therefore, in this research 10 paint samples (blue and red) from the five manuscripts related to Safavid period (16th century) were analyzed to explore their nature and structure. First, the related literature regarding the frequent types of the paints in Safavid period and their preparing recipe were thoroughly reviewed. Then, after sampling of the paints, the analytical techniques including scanning electron microscopy-energy dispersive X-ray spectroscopy (SEM-EDX) and Fourier transform infrared spectroscopy (FTIR) were used to identify red and blue pigments structure. Obtained results confirmed that all the used red and blue pigments in these five manuscripts were of mineral origin. Moreover, the results proved that all of the red pigments used in this manuscript were of vermilion, ocher and red lead (Lead oxide), while the blue pigments are of ultramarine type. Also, the strong peak of FTIR at 2340 cm-1 proved that the ultramarine pigment used is of natural type.

Elahe Pourabdollah,
Volume 4, Issue 1 (10-2021)
Abstract

Pigments play a crucial role in identifying the authenticity of historical and cultural artworks and hold a special position in conservation and restoration practices. Among them, recognizing the methods of identifying pigments used in historical manuscripts plays a significant role in determining the identity and authenticity of these artifacts. This study aims to review various methods of identifying pigments employed in historical manuscripts. Investigations in this paper have been conducted using non-destructive analytical techniques such as Scanning Electron
Microscope with Energy Dispersive X-ray Spectroscopy (SEM-EDX), Fourier Transform Infrared Spectroscopy (FTIR), X-ray Fluorescence (XRF), X-ray Diffraction (XRD), Polarized Light Microscopy (PLM), Particle Induced X-ray Emission (PIXE), Atomic Force Microscopy (AFM), micro-Raman spectroscopy, and optical imaging for elemental and compositional identification of pigments. Among these methods, SEM-EDX and point analysis
have been more commonly used in identifying historical pigments. Additionally, the combination of multiple techniques can be a suitable solution for identification purposes, but depending on the purpose of identification and the sensitivity of the artifact, factors such as the feasibility of on-site analysis or transferring artifacts to various laboratory facilities, using non-destructive methods, the possibility of sampling, and the significance and value of the artifact should be considered to adopt the best possible method. If necessary, combining tests and instrumental methods can lead to a more accurate understanding of pigments alongside their chemical composition.

Shiva Razavi,
Volume 5, Issue 3 (12-2022)
Abstract

Pottery is one of the artistic-technical craft that has persisted for several millennia from prehistoric times to the present day. Such artifacts, particularly in Iran, exhibit high stylistic and technological diversity. In most archaeological excavations, consistently various types of these artifacts from different historical periods and styles have been discovered, whose technical study and form recovery can provide valuable information to researchers in various fields. Among these excavations is the Tappeh-Silveh in Piranshahr, where diverse pottery dating back to the Chalcolithic, Early Bronze Age, Iron Age, as well as remnants from the Parthian period and the subsequent Islamic period have been uncovered. The specimen studied in this article is a decorated orange pottery piece with black and red colors and geometric patterns, belonging to the Bronze Age from this site. This piece has sustained damages such as fractures, losses, and deposits, , which have been improperly repaired. It requires cleaning, reattachment, and reconstruction of the missing parts, while adhering to the theoretical principles of conservation. Accordingly, after necessary pathological and technical studies of the artifact using laboratory methods, an appropriate cleaning method was selected, and essential actions were taken towards its protection and restoration.


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